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alekya guggilam  
#1 Posted : 17 March 2014 16:35:53(UTC)
Rank: New forum user
alekya guggilam

I am writing down safe systems of work for my company and I am struggling to complete one of them: Drying of samples ( pieces of rock) after exposure to solvents . At the moment we air dry the samples and then put them into the oven at a set temperature. But I am not satisfied with air drying of samples as I am unsure if the solvent level in the samples is below LEL (Lower explosion limit) prior to putting them into the oven. Could anyone please advise a safe method to remove solvents from samples after solvent cleaning considering the below: • Staff must not be exposed to high levels of solvent vapours • Must not create explosive atmosphere • Any situation which may lead risk to health, safety or environment Thank you, Alekya
Steve e ashton  
#2 Posted : 17 March 2014 18:17:14(UTC)
Rank: Super forum user
Steve e ashton

Do you have any data on the weights of samples before and after oven drying? If you know how much solvent is going into the oven, and how long it is taking to flash off or boil away then you (or someone else) should be able to calculate the likely solvent loading and decide whether you need to add ventilation to the oven.... Plus, it depends on what the solvent is, and how long it takes to evaporate. What its flashpoint is, and how deeply it may be absorbed into the sample... A client was recently issued a material breach notice for failure to have a DSEAR assessment available for (amongst other things) an oven which was drying inks and paints from small components. Long story short - there was, and could never have been, any risk of significant fire or explosion in the oven (components introduced slowly on a conveyor, minute levels of solvent. forced air ventilation, system interlocks etc etc....).
alekya guggilam  
#3 Posted : 19 March 2014 11:35:11(UTC)
Rank: New forum user
alekya guggilam

I don't have weights of the sample before and after drying. I will try get this information.
Jane Blunt  
#4 Posted : 19 March 2014 12:17:56(UTC)
Rank: Super forum user
Jane Blunt

Can you tell us what the solvents are and the temperature of the oven as well?
boblewis  
#5 Posted : 19 March 2014 12:47:52(UTC)
Rank: Super forum user
boblewis

I tend to prefer Vacuum Drying in such situations as any potential for fire/explosion is significantly eliminated. Remember the hierarchy of risk control. You can readily monitor the exhaust gases for VOC levels. Bob
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